Course Description
| Course | Code | Semester | T+P (Hour) | Credit | ECTS |
|---|---|---|---|---|---|
| ANALYTICAL CHEMISTRY II | - | Spring Semester | 3+0 | 3 | 5 |
| Course Program |
| Prerequisites Courses | |
| Recommended Elective Courses |
| Language of Course | English |
| Course Level | First Cycle (Bachelor's Degree) |
| Course Type | Required |
| Course Coordinator | Assist.Prof. Sema KOYUTÜRK |
| Name of Lecturer(s) | Assist.Prof. Ümit Can ERİM, Assist.Prof. Sema KOYUTÜRK |
| Assistant(s) | Research assistant of faculty |
| Aim | To be able to do qualitative and quantitative chemical analysis to make the students gain knowledge and skills by teaching fundamentals of instrumental analysis techniques in addition to the analytical chemistry and electrochemistry. |
| Course Content | This course contains; Complexation reactions and titrations,Electrochemistry,The applications of oxidation-reduction titrations,Potentiometry,Potentiometry applications,Electrogravimetry and coulometry,Voltammetry,Introduction to spectrochemical methods,Molecular absorption spectroscopy,Molecular absorption spectroscopy,Molecular fluorescence spectroscopy,Introduction to chromatographic methods,Gas chromatography,High-performance liquid chromatography. |
| Dersin Öğrenme Kazanımları | Teaching Methods | Assessment Methods |
| 1. Discusses the complexation reactions, application of them to titration procedures and obtained results. | 10, 12, 16, 9 | A |
| 1.1. Applies the complex formation reactions to titration method. | 10, 12, 16, 9 | A |
| 1.2. Explains the reaction of some organic complexation reagents. | 10, 12, 16, 9 | A |
| 1.3. Interprets the results of the analysis and EDTA titration technique. | 10, 12, 16, 9 | A |
| 2. Discusses the electrode potentials, electrochemistry of oxidation-reduction reactions and the basic principles of electrochemistry. | 10, 12, 16, 9 | A |
| 2.1. Interprets the basic principles of electrochemistry. | 10, 12, 16, 9 | A |
| 2.2. Electrochemically explains the oxidation-reduction reactions. | 10, 12, 16, 9 | A |
| 2.3. Interprets the electrochemical cells and electrode potentials. | 10, 12, 16, 9 | A |
| 3. Discusses the applications of oxidation-reduction titration and properties of the materials used in this method. | 10, 12, 16, 9 | A |
| 3.1. Interprets the applications of oxidation-reduction titration | 10, 12, 16, 9 | A |
| 3.2. Explains the properties of standard reducing and oxidizing substances used in this titration technique. | 10, 12, 16, 9 | A |
| 4. Discusses the applications of potentiometric titration, electrodes used in potentiometry and basic principles of potentiometry. | 10, 12, 16, 9 | A |
| 4.1. Explains the basic principles of potentiometry. | 10, 12, 16, 9 | A |
| 4.2. Interprets the calculations and applications of potentiometric titration. | 10, 12, 16, 9 | A |
| 5. Discusses the electrogravimetric, coulometric and voltammetric methods with the basic principles of electrogravimetry, coulometry and voltammetry. | 10, 12, 16, 9 | A |
| 5.1. Interprets the basic principles of electrogravimetry and coulometry. | 10, 12, 16, 9 | A |
| 5.2. Explains the effect of current to the cell potential. | 10, 12, 16, 9 | A |
| 5.3. Interprets the electrogravimetric and coulometric methods. | 10, 12, 16, 9 | A |
| 5.4. Explains the stripping methods, linear scanning voltammetry, pulse polarographic and voltammetric methods. | 10, 12, 16, 9 | A |
| 6. Discusses the absorption and emission of the light, electromagnetic spectrum, electromagnetic radiation which are constituents of spectrochemical methods. | 10, 12, 16, 9 | A |
| 6.1. Explains the general properties of electromagnetic radiation. | 10, 12, 16, 9 | A |
| 6.2. Interprets the electromagnetic spectrum, absorption and emission of the light. | 10, 12, 16, 9 | A |
| 7. Discusses application techniques and the fundamental principles of molecular absorption spectroscopy and molecular fluorescence spectroscopy. | 10, 12, 16, 9 | A |
| 7.1. Explains the infrared spectroscopy, ultraviolet and visible molecular absorption spectroscopy. | 10, 12, 16, 9 | A |
| 7.2. Interprets the applications of fluorescence methods and the theory of molecular fluorescence. | 10, 12, 16, 9 | A |
| 8. Discusses the applications of high-performance liquid chromatography, gas chromatography and basic principles of chromatographic methods. | 10, 12, 16, 9 | A |
| 8.1. Explains the applications of gas-liquid chromatography and gas chromatography columns. | 10, 12, 16, 9 | A |
| 8.2. Explains the high performance partition chromatography, adsorption, ion exchange and size exclusion chromatographic methods. | 10, 12, 16, 9 | A |
| 8.3. Compares high performance liquid chromatography and gas-liquid chromatography and interprets the supercritical fluid chromatography and planer chromatography. | 10, 12, 16, 9 | A |
| Teaching Methods: | 10: Discussion Method, 12: Problem Solving Method, 16: Question - Answer Technique, 9: Lecture Method |
| Assessment Methods: | A: Traditional Written Exam |
Course Outline
| Order | Subjects | Preliminary Work |
|---|---|---|
| 1 | Complexation reactions and titrations | 1, 2, 3 |
| 2 | Electrochemistry | 1, 2, 3 |
| 3 | The applications of oxidation-reduction titrations | 1, 2, 3 |
| 4 | Potentiometry | 1, 2, 3 |
| 5 | Potentiometry applications | 1, 2, 3 |
| 6 | Electrogravimetry and coulometry | 1, 2, 3 |
| 7 | Voltammetry | 1, 2, 3 |
| 8 | Introduction to spectrochemical methods | 1, 2, 3 |
| 9 | Molecular absorption spectroscopy | 1, 2, 3 |
| 10 | Molecular absorption spectroscopy | 1, 2, 3 |
| 11 | Molecular fluorescence spectroscopy | 1, 2, 3 |
| 12 | Introduction to chromatographic methods | 1, 2, 3 |
| 13 | Gas chromatography | 1, 2, 3 |
| 14 | High-performance liquid chromatography | 1, 2, 3 |
| Resources |
| [1] Kılıç, E., Köseoğlu, F., (Çeviri editörleri), (Skoog, D. A., West, D. M., Holler F.J., Crouch, S.R.,) Analitik Kimya, Cilt 1, Bilim Yayıncılık, 8. Baskı, Ankara, 2009. [2] Kılıç, E., Köseoğlu, F., (Çeviri editörleri), (Skoog, D. A., West, D. M., Holler F.J., Crouch, S.R.,) Analitik Kimya, Cilt 2, Bilim Yayıncılık, 8. Baskı, Ankara, 2009. |
| [3] Gündüz, T. Kantitatif Analiz Ders Kitabı, Gazi Kitabevi, 7. Baskı, Ankara, 2003. |
Course Contribution to Program Qualifications
| Course Contribution to Program Qualifications | |||||||
| No | Program Qualification | Contribution Level | |||||
| 1 | 2 | 3 | 4 | 5 | |||
| 1 | PQ-1. Skilfully use information technology to access, follow, evaluate and apply current knowledge in the field of Pharmaceutical Sciences. | X | |||||
| 2 | PQ-2. Have advanced knowledge in APIs and DPs. | ||||||
| 3 | PQ-3. Collaborate with the experts for collection, interpretation, application and declaration of data in Pharmaceutical Sciences field. | X | |||||
| 4 | PQ-4. Provide best patient counseling services and medication therapy management using his/her knowledge and pharmaceutical information systems to improve the quality of life and safety of patient. | ||||||
| 5 | PQ-5. Capable of organizing and administering a drugstore as per responsibilities prescribed under the Pharmacy Law, using skills, knowledge and advanced technology systems. | ||||||
| 6 | PQ-6. Skilfully use computer programs and advanced technology related to the Pharmaceutical Sciences. | ||||||
| 7 | PQ-7. Provide solutions to the professional issues using scientific knowledge and data. | X | |||||
| 8 | PQ-8. Perform identification, quality control and standardization of the drug products. | X | |||||
| 9 | PQ-9. Prepare and implement developmental plans for his/her subordinates, frequently evaluate their progress and make necessary adjustments. | X | |||||
| 10 | PQ-10. Capable of conducting independent studies with his/her advanced knowledge in pharmaceutical sciences, takes responsibilities in professional organizations and efficiently collaborates with the members of his/her own organization as well as other organizations. | X | |||||
| 11 | PQ-11. Clearly show signs of adoption of life-long learning and openness to further development. | X | |||||
| 12 | PQ-12. Critically evaluate their knowledge in pharmaceutical sciences. | X | |||||
| 13 | PQ-13. Closely follow and evaluate the national and international professional developments. | ||||||
| 14 | PQ-14. Record and document all professional activities and applications. | X | |||||
| 15 | PQ-15. Communicate all necessary information about medicines to patient, medical personnel and public. | ||||||
| 16 | PQ-16. Proficient in English to communicate and follow current knowledge in pharmaceutical sciences. | ||||||
| 17 | PQ-17. Inform officials and organizations about the issues with the quality assurance of pharmaceutical products. | X | |||||
| 18 | PQ-18. Actively involve in the preparation of APIs, every stage of the formulation and production of DPs. | X | |||||
| 19 | PQ-19. Knowledgable in the regulatory rules of new drug application, data protection and patent issues and understand their interrelationship. | ||||||
| 20 | PQ-20. Have awareness of his/her duties, rights and responsibilities and act based on Pharmacy Law and high professional ethical standards. | X | |||||
| 21 | PQ-21. Familiar with and actively pursue the personal and public health, environmental, and work safety issues. | X | |||||
Assessment Methods
| Contribution Level | Absolute Evaluation | |
| Rate of Midterm Exam to Success | 40 | |
| Rate of Final Exam to Success | 60 | |
| Total | 100 | |
| ECTS / Workload Table | ||||||
| Activities | Number of | Duration(Hour) | Total Workload(Hour) | |||
| Course Hours | 14 | 3 | 42 | |||
| Guided Problem Solving | 14 | 2 | 28 | |||
| Resolution of Homework Problems and Submission as a Report | 14 | 1 | 14 | |||
| Term Project | 0 | 0 | 0 | |||
| Presentation of Project / Seminar | 0 | 0 | 0 | |||
| Quiz | 0 | 0 | 0 | |||
| Midterm Exam | 1 | 31 | 31 | |||
| General Exam | 1 | 41 | 41 | |||
| Performance Task, Maintenance Plan | 0 | 0 | 0 | |||
| Total Workload(Hour) | 156 | |||||
| Dersin AKTS Kredisi = Toplam İş Yükü (Saat)/30*=(156/30) | 5 | |||||
| ECTS of the course: 30 hours of work is counted as 1 ECTS credit. | ||||||
Detail Informations of the Course
Course Description
| Course | Code | Semester | T+P (Hour) | Credit | ECTS |
|---|---|---|---|---|---|
| ANALYTICAL CHEMISTRY II | - | Spring Semester | 3+0 | 3 | 5 |
| Course Program |
| Prerequisites Courses | |
| Recommended Elective Courses |
| Language of Course | English |
| Course Level | First Cycle (Bachelor's Degree) |
| Course Type | Required |
| Course Coordinator | Assist.Prof. Sema KOYUTÜRK |
| Name of Lecturer(s) | Assist.Prof. Ümit Can ERİM, Assist.Prof. Sema KOYUTÜRK |
| Assistant(s) | Research assistant of faculty |
| Aim | To be able to do qualitative and quantitative chemical analysis to make the students gain knowledge and skills by teaching fundamentals of instrumental analysis techniques in addition to the analytical chemistry and electrochemistry. |
| Course Content | This course contains; Complexation reactions and titrations,Electrochemistry,The applications of oxidation-reduction titrations,Potentiometry,Potentiometry applications,Electrogravimetry and coulometry,Voltammetry,Introduction to spectrochemical methods,Molecular absorption spectroscopy,Molecular absorption spectroscopy,Molecular fluorescence spectroscopy,Introduction to chromatographic methods,Gas chromatography,High-performance liquid chromatography. |
| Dersin Öğrenme Kazanımları | Teaching Methods | Assessment Methods |
| 1. Discusses the complexation reactions, application of them to titration procedures and obtained results. | 10, 12, 16, 9 | A |
| 1.1. Applies the complex formation reactions to titration method. | 10, 12, 16, 9 | A |
| 1.2. Explains the reaction of some organic complexation reagents. | 10, 12, 16, 9 | A |
| 1.3. Interprets the results of the analysis and EDTA titration technique. | 10, 12, 16, 9 | A |
| 2. Discusses the electrode potentials, electrochemistry of oxidation-reduction reactions and the basic principles of electrochemistry. | 10, 12, 16, 9 | A |
| 2.1. Interprets the basic principles of electrochemistry. | 10, 12, 16, 9 | A |
| 2.2. Electrochemically explains the oxidation-reduction reactions. | 10, 12, 16, 9 | A |
| 2.3. Interprets the electrochemical cells and electrode potentials. | 10, 12, 16, 9 | A |
| 3. Discusses the applications of oxidation-reduction titration and properties of the materials used in this method. | 10, 12, 16, 9 | A |
| 3.1. Interprets the applications of oxidation-reduction titration | 10, 12, 16, 9 | A |
| 3.2. Explains the properties of standard reducing and oxidizing substances used in this titration technique. | 10, 12, 16, 9 | A |
| 4. Discusses the applications of potentiometric titration, electrodes used in potentiometry and basic principles of potentiometry. | 10, 12, 16, 9 | A |
| 4.1. Explains the basic principles of potentiometry. | 10, 12, 16, 9 | A |
| 4.2. Interprets the calculations and applications of potentiometric titration. | 10, 12, 16, 9 | A |
| 5. Discusses the electrogravimetric, coulometric and voltammetric methods with the basic principles of electrogravimetry, coulometry and voltammetry. | 10, 12, 16, 9 | A |
| 5.1. Interprets the basic principles of electrogravimetry and coulometry. | 10, 12, 16, 9 | A |
| 5.2. Explains the effect of current to the cell potential. | 10, 12, 16, 9 | A |
| 5.3. Interprets the electrogravimetric and coulometric methods. | 10, 12, 16, 9 | A |
| 5.4. Explains the stripping methods, linear scanning voltammetry, pulse polarographic and voltammetric methods. | 10, 12, 16, 9 | A |
| 6. Discusses the absorption and emission of the light, electromagnetic spectrum, electromagnetic radiation which are constituents of spectrochemical methods. | 10, 12, 16, 9 | A |
| 6.1. Explains the general properties of electromagnetic radiation. | 10, 12, 16, 9 | A |
| 6.2. Interprets the electromagnetic spectrum, absorption and emission of the light. | 10, 12, 16, 9 | A |
| 7. Discusses application techniques and the fundamental principles of molecular absorption spectroscopy and molecular fluorescence spectroscopy. | 10, 12, 16, 9 | A |
| 7.1. Explains the infrared spectroscopy, ultraviolet and visible molecular absorption spectroscopy. | 10, 12, 16, 9 | A |
| 7.2. Interprets the applications of fluorescence methods and the theory of molecular fluorescence. | 10, 12, 16, 9 | A |
| 8. Discusses the applications of high-performance liquid chromatography, gas chromatography and basic principles of chromatographic methods. | 10, 12, 16, 9 | A |
| 8.1. Explains the applications of gas-liquid chromatography and gas chromatography columns. | 10, 12, 16, 9 | A |
| 8.2. Explains the high performance partition chromatography, adsorption, ion exchange and size exclusion chromatographic methods. | 10, 12, 16, 9 | A |
| 8.3. Compares high performance liquid chromatography and gas-liquid chromatography and interprets the supercritical fluid chromatography and planer chromatography. | 10, 12, 16, 9 | A |
| Teaching Methods: | 10: Discussion Method, 12: Problem Solving Method, 16: Question - Answer Technique, 9: Lecture Method |
| Assessment Methods: | A: Traditional Written Exam |
Course Outline
| Order | Subjects | Preliminary Work |
|---|---|---|
| 1 | Complexation reactions and titrations | 1, 2, 3 |
| 2 | Electrochemistry | 1, 2, 3 |
| 3 | The applications of oxidation-reduction titrations | 1, 2, 3 |
| 4 | Potentiometry | 1, 2, 3 |
| 5 | Potentiometry applications | 1, 2, 3 |
| 6 | Electrogravimetry and coulometry | 1, 2, 3 |
| 7 | Voltammetry | 1, 2, 3 |
| 8 | Introduction to spectrochemical methods | 1, 2, 3 |
| 9 | Molecular absorption spectroscopy | 1, 2, 3 |
| 10 | Molecular absorption spectroscopy | 1, 2, 3 |
| 11 | Molecular fluorescence spectroscopy | 1, 2, 3 |
| 12 | Introduction to chromatographic methods | 1, 2, 3 |
| 13 | Gas chromatography | 1, 2, 3 |
| 14 | High-performance liquid chromatography | 1, 2, 3 |
| Resources |
| [1] Kılıç, E., Köseoğlu, F., (Çeviri editörleri), (Skoog, D. A., West, D. M., Holler F.J., Crouch, S.R.,) Analitik Kimya, Cilt 1, Bilim Yayıncılık, 8. Baskı, Ankara, 2009. [2] Kılıç, E., Köseoğlu, F., (Çeviri editörleri), (Skoog, D. A., West, D. M., Holler F.J., Crouch, S.R.,) Analitik Kimya, Cilt 2, Bilim Yayıncılık, 8. Baskı, Ankara, 2009. |
| [3] Gündüz, T. Kantitatif Analiz Ders Kitabı, Gazi Kitabevi, 7. Baskı, Ankara, 2003. |
Course Contribution to Program Qualifications
| Course Contribution to Program Qualifications | |||||||
| No | Program Qualification | Contribution Level | |||||
| 1 | 2 | 3 | 4 | 5 | |||
| 1 | PQ-1. Skilfully use information technology to access, follow, evaluate and apply current knowledge in the field of Pharmaceutical Sciences. | X | |||||
| 2 | PQ-2. Have advanced knowledge in APIs and DPs. | ||||||
| 3 | PQ-3. Collaborate with the experts for collection, interpretation, application and declaration of data in Pharmaceutical Sciences field. | X | |||||
| 4 | PQ-4. Provide best patient counseling services and medication therapy management using his/her knowledge and pharmaceutical information systems to improve the quality of life and safety of patient. | ||||||
| 5 | PQ-5. Capable of organizing and administering a drugstore as per responsibilities prescribed under the Pharmacy Law, using skills, knowledge and advanced technology systems. | ||||||
| 6 | PQ-6. Skilfully use computer programs and advanced technology related to the Pharmaceutical Sciences. | ||||||
| 7 | PQ-7. Provide solutions to the professional issues using scientific knowledge and data. | X | |||||
| 8 | PQ-8. Perform identification, quality control and standardization of the drug products. | X | |||||
| 9 | PQ-9. Prepare and implement developmental plans for his/her subordinates, frequently evaluate their progress and make necessary adjustments. | X | |||||
| 10 | PQ-10. Capable of conducting independent studies with his/her advanced knowledge in pharmaceutical sciences, takes responsibilities in professional organizations and efficiently collaborates with the members of his/her own organization as well as other organizations. | X | |||||
| 11 | PQ-11. Clearly show signs of adoption of life-long learning and openness to further development. | X | |||||
| 12 | PQ-12. Critically evaluate their knowledge in pharmaceutical sciences. | X | |||||
| 13 | PQ-13. Closely follow and evaluate the national and international professional developments. | ||||||
| 14 | PQ-14. Record and document all professional activities and applications. | X | |||||
| 15 | PQ-15. Communicate all necessary information about medicines to patient, medical personnel and public. | ||||||
| 16 | PQ-16. Proficient in English to communicate and follow current knowledge in pharmaceutical sciences. | ||||||
| 17 | PQ-17. Inform officials and organizations about the issues with the quality assurance of pharmaceutical products. | X | |||||
| 18 | PQ-18. Actively involve in the preparation of APIs, every stage of the formulation and production of DPs. | X | |||||
| 19 | PQ-19. Knowledgable in the regulatory rules of new drug application, data protection and patent issues and understand their interrelationship. | ||||||
| 20 | PQ-20. Have awareness of his/her duties, rights and responsibilities and act based on Pharmacy Law and high professional ethical standards. | X | |||||
| 21 | PQ-21. Familiar with and actively pursue the personal and public health, environmental, and work safety issues. | X | |||||
Assessment Methods
| Contribution Level | Absolute Evaluation | |
| Rate of Midterm Exam to Success | 40 | |
| Rate of Final Exam to Success | 60 | |
| Total | 100 | |